● Synthesis reactor at laboratory scale
Study of the various unit operations identified
Inorganic and organic chemical reactions
Evaporation at atmospheric pressure or under vacuum
Crystallization by controlled cooling
Static decanting
Select and study the influence of process parameters such as
Service pressure: vacuum or atmospheric pressure
Stirring speed
Heating temperature
Cooling process
General specifications
● 3 L, SS tank, double jacket, glass cover.
● Stirring system, speed display, PTFE coated SS stirring shaft, PTFE three‐blade propeller.
● Graduated glass feeding funnel, 1 L.
● Reflux head and monobloc cooler, glass coil, manual reflux valve.
● Glass coil exchanger.
● Two glass receivers for distillate, gradu‐ ated 1L.
● Heating unit.
● Glass vacuum trap.
Instrumentation
● SS thermometer inox 316 L.
● Digital Thermometer for reflux head.
● Vacuum manometer.
● Flowmeter.
Options
‐Buchner Filter
‐Vacuum Pump
Chemical engineering refers especially to chemical reaction engineering. Indeed, chemical reactions, catalyzed or not, are at the heart of all industrial syntheses.
Study of a chemical reaction, in a perfectly‐stirred reactor, permits the operator to understand the influence of the different parameters in the optimization of the chemical synthesis with a view to its industrialization.
