● Multipurpose unit for :
Liquid‐liquid mixture
Solid‐Liquid dissolution
Evaporation, concentration
Reaction, synthesis
Distillation
Decantation, crystallization
● Heating by steam generator
● Cooling by water circulation inside the double jacket
Operator training to monitor the process
Unit placed under vacuum
Compliance with procedures
Loading through the dropping funnel
Receivers draining under vacuum
Phenomena viewing
Synoptic follow
Curves using
Unit cleaning
Handling report
Follow ‐ up of reaction kinetics
Kinetic, material balance, reaction yield
Separation of the products
By distillation, decantation or crystallization
General specifications
● Jacketed SS vessel, and SS flat cover.
● Variable speed stirrer.
● Glass feeding vessel.
● Glass distillation column, SS Multiknit packing.
● Reflux divider with PTFE pneumatic valve.
● Glass calendar condenser and SS coil.
● Glass azeotropic decanter , glass double jacket.
● SS distillate cooler.
● Two graduated glass receivers, 2L, three ways selecting valve, setting, vent and draining valves.
● Vacuum circuit with vacuum trap.
● Vacuum pump.
● Cold water circuit.
● Steam circuit : with solenoid valve, insulated pipes.
● Steam generator.
Instrumentation
● 5 temperature probes Pt100Ω.
● 3 flowmeters:.
● Vacuum manometer.
● Solenoid valve on steam circuit. Safety
● Discharge check valve.
● Motor coupling and reactor protection.
● Steam cut off in case of emergency.
