● Study of the batch distillation
Glass spherical boiler
Perforate plates column
Internal reflux
Influence of operating parameters
Reflux ratio, boiler heating capacity, quality of mixture to be distilled
Batch distillation
Materials balance
Monitoring of liquid‐vapor equilibrium and temperatures
Yield, productivity
General specifications
• Glass boiler vessel 2L , with draining valve.
• Heating mantle, protection by insulation and SS sheet.
• Distillation column with perforated plates, sampling valve.
• Glass reflux divider, glass distillate drain‐ ing out by a solenoid acting a magnetic valve.
• Glass condenser, glass coil.
• SS cooler.
• Glass distillate receiver, 1 L.
• Cool water circuit.
Instrumentation
• 6 temperature probes Pt100Ω.
• Flowmeter.
