● Separation industrial process implementation
● Continuous distillation study under atmospheric pressure
Operating training learning
Unit start study
Determination of an operating point
Controls configuration
Transitory phase study
Study of the different types of control : level, temperature, flow, pressure
Influence of the operating parameters
Heating power
Feed rate
Feeding solution concentration
Feeding level
Reflux ratio
Perfom a continuous process
Mass and thermal balance, yield
General specifications
● 30L polyethylene tank. Draining valve.
● 2 gear pumps SS/PEEK head, with integrated safety valve.
● SS preheater.
● 6L max. glass thermosiphon boiler, SS heating element.
● Glass column, removable insulating, glass bubble cap trays, SS intermediary trays.
● Glass condenser, SS coil.
● Glass refrigerant, sampling valve.
● 2 graduated glass vessels, solenoid valve.
● 2 polyethylene tank, 10L.
● Cold water circuit.
● SS spill containment tray, draining valve.
Safety
‐ Venting thermostate.
‐ Pressure relief on the heating line.
Instrumentation
● Temperature probes Pt 100Ω.
● 1 safety thermostat.
● 1 vane flow transmitter.
● 1 water flow transmitter.
● 1 ethanol flow transmitter.
● 3 electronic relative pressure transmitters. 1 electronic differential pressure trans‐ mitter.
● 3 level detectors.
